CAS： 937371-89-6
A non-aqueous inkjet ink includes C.I. P...
2,9-dichloroquinacridone
dimethyl 5-chloromethyl-1,3-benzenedicarboxylate
QAD-3
| Conditions | Yield |
|---|---|
|
2,9-dichloroquinacridone;
With
potassium tert-butylate;
In
dimethyl sulfoxide;
at 110 ℃;
for 1h;
dimethyl 5-chloromethyl-1,3-benzenedicarboxylate;
In
dimethyl sulfoxide;
at 40 ℃;
for 4h;
|
100% |
1,3,5-tris-(methoxycarbonyl)benzene
QAD-3
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1.1: lithium borohydride / acetic acid methyl ester; tetrahydrofuran / 3 h / 50 °C
2.1: thionyl chloride / N,N-dimethyl acetamide / toluene / 4 h / 40 °C
3.1: potassium tert-butylate / dimethyl sulfoxide / 1 h / 110 °C
3.2: 4 h / 40 °C
With
lithium borohydride; thionyl chloride; potassium tert-butylate;
N,N-dimethyl acetamide;
In
tetrahydrofuran; acetic acid methyl ester; dimethyl sulfoxide; toluene;
|
1,3,5-tris-(methoxycarbonyl)benzene
2,9-dichloroquinacridone
dimethyl 5-chloromethyl-1,3-benzenedicarboxylate
dimethyl 5-hydroxymethylbenzene-1,3-dicarboxylate