3-Nitrocatechol

Base Information

  • PRODUCT:3-Nitrocatechol
  • CAS.:6665-98-1
  • MF:C6H5 N O4
  • Molecular Weight:155.11
  • Purity:99%

Product Details

CAS: 6665-98-1

MF: C6H5 N O4

Buy cost-effective 99% pure 3-Nitrocatechol 6665-98-1 now

  • Molecular Formula:C6H5 N O4
  • Molecular Weight:155.11
  • Vapor Pressure:0.00461mmHg at 25°C 
  • Refractive Index:1.5423 (estimate) 
  • Boiling Point:268.6°C at 760 mmHg 
  • Flash Point:123.7°C 
  • PSA:86.28000 
  • Density:1.58g/cm3 
  • LogP:1.52920 

3-Nitrocatechol(Cas 6665-98-1) Usage

InChI:InChI=1/C6H5NO4/c8-5-3-1-2-4(6(5)9)7(10)11/h1-3,8-9H

6665-98-1 Relevant articles

Gas-phase IR cross-sections and single crystal structures data for atmospheric relevant nitrocatechols

Arsene, Cecilia,Bejan, Iustinian-Gabriel,Olariu, Romeo-Iulian,Roman, Claudiu,Roman, Tiberiu

, (2021/09/28)

The gas-phase IR absorption cross sectio...

Cystobactamid 507: Concise Synthesis, Mode of Action, and Optimization toward More Potent Antibiotics

Elgaher, Walid A. M.,Hamed, Mostafa M.,Baumann, Sascha,Herrmann, Jennifer,Siebenbürger, Lorenz,Krull, Jana,Cirnski, Katarina,Kirschning, Andreas,Br?nstrup, Mark,Müller, Rolf,Hartmann, Rolf W.

supporting information, p. 7219 - 7225 (2020/05/08)

Lack of new antibiotics and increasing a...

Class of large ring heterocyclic compound restraining HCV and manufacturing and uses thereof

-

Paragraph 0278; 0279; 0280; 0281, (2017/09/01)

The invention relates to a class of comp...

Microwave assisted synthesis of nitro phenols from the reaction of phenols with urea nitrate under acid-free conditions

Verma, Sanny,Pandita, Sangeeta,Jain, Suman L.

, p. 1320 - 1322 (2014/03/21)

Urea nitrate was found to be an inexpens...

6665-98-1 Process route

1-nitro-1-phenylmethane
622-42-4

1-nitro-1-phenylmethane

sodium carbonate monohydrate

sodium carbonate monohydrate

3-nitrobenzene-1,2-diol
6665-98-1

3-nitrobenzene-1,2-diol

2-nitro-2-phenyl-propane-1,3-diol
5428-02-4

2-nitro-2-phenyl-propane-1,3-diol

Conditions
Conditions Yield
With formaldehyd; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; toluene;
78%
With formaldehyd; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; toluene;
78%
With formaldehyd; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; toluene;
78%
benzene-1,2-diol
120-80-9,19481-10-8,37349-32-9

benzene-1,2-diol

3-nitrobenzene-1,2-diol
6665-98-1

3-nitrobenzene-1,2-diol

Conditions
Conditions Yield
With uronium nitrate; In water; acetonitrile; at 80 ℃; for 0.5h; regioselective reaction; Microwave irradiation;
75%
With copper(II) nitrate/zeolite H-Y; at 70 - 80 ℃; for 2h; Further Variations:; heating mode; times; Product distribution;
65%
With nitric acid; In diethyl ether; at 0 - 20 ℃; for 24h; Cooling with ice;
50%
With nitric acid; In diethyl ether; at 0 - 20 ℃;
31.2%
With nitric acid; In diethyl ether; at 0 - 20 ℃; for 0.333333h;
30%
With diethyl ether; nitric acid;
durch Nitrierung;
Multi-step reaction with 3 steps
1: aqueous sodium carbonate-solution; sodium dithionite
2: aqueous nitric acid; acetic acid / 30 - 35 °C
3: ethanolic KOH
With potassium hydroxide; sodium dithionite; nitric acid; sodium carbonate; acetic acid;
With conc. nitric acid; In Petroleum ether;
With nitric acid;
With nitric acid; In diethyl ether;
With nitric acid; In diethyl ether; at 20 ℃; for 0.333333h;
With nitric acid; In diethyl ether; for 0.5h;

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